Ultrasound Assisted Synthesis and Characterization of Mn Doped CdS Nanocrystalline Zinc-Blendes
نویسندگان
چکیده مقاله:
Cd1-xMnxS (x = 0, 0.1, 0.2) nanoparticles, prepared by co-precipitation method under ultrasonic irradiation, were studied by means of X-ray diffraction, scanning electron microscopy, FTIR and UV-Vis spectroscopy measurements. The average particle size of nanoparticles from the scanning electron microscopy image is about 20-30 nm. Results show that partial substitution of Cd by Mn leads to a reduction in lattice parameters and enhancement of band gap energy. This is attributed to the nanometric grain size and quantum confinement effects. The particle size is calculated to be around 2 nm that is almost in agreement with the crystallite size estimated from the XRD result.
منابع مشابه
ultrasound assisted synthesis and characterization of mn doped cds nanocrystalline zinc-blendes
cd1-xmnxs (x = 0, 0.1, 0.2) nanoparticles, prepared by co-precipitation method under ultrasonic irradiation, were studied by means of x-ray diffraction, scanning electron microscopy, ftir and uv-vis spectroscopy measurements. the average particle size of nanoparticles from the scanning electron microscopy image is about 20-30 nm. results show that partial substitution of cd by mn leads to a re...
متن کاملUltrasound Assisted Green Synthesis and Characterization of Graphene Oxide
Graphene oxide (GO) was prepared by an improved green chemical method using graphite flakes, KMnO4, a mixture of H2SO4/H3PO4, H2O2 and HCl. In several stages, ultrasound was used to separate the oxidized layers of GO. The use of ultrasound optimizes the effect of the reacting agents, decreasing the required amou...
متن کاملSynthesis and local structure of doped nanocrystalline zinc oxides
Nanocrystalline zinc oxides are produced by chemical vapor synthesis and characterized by x-ray diffraction, high resolution transmission electron microscopy, nitrogen sorption, and extended x-ray absorption fine structure. Dopant elements aluminum, gallium, and indium influence the particle size of the powders as well as lattice parameters and local structure. The different effects of the thre...
متن کاملsynthesis and characterization of some macrocyclic schiff bases
ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...
15 صفحه اولSynthesis and Characterization of Hexagonal Shaped Nanocrystalline Zinc Oxide Powders
Nanocrystalline ZnO powders are synthesized using a quick, simple and inexpensive combustion method. Glycine and zinc nitrate, used as fuel and oxidant/cation sources respectively, were mixed together at room temperature to form a slurry or gel. A series of experiments were performed to synthesize nanoparticles for different fuel to oxidant ratios. The rate of heating and stirring greatly influ...
متن کاملSynthesis and Characterization of Mn-Doped ZnO Nanocrystals.
We report the synthesis and characterization of several sizes of Mn-doped ZnO nanocrystals, both in the free-standing and the capped particle forms. The sizes of these nanocrystals could be controlled by capping them with polyvinylpyrollidone under different synthesis conditions and were estimated by X-ray diffraction and transmission electron microscopy. The absorption properties of PVP-capped...
متن کاملمنابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
ذخیره در منابع من قبلا به منابع من ذحیره شده{@ msg_add @}
عنوان ژورنال
دوره 5 شماره 4
صفحات 375- 383
تاریخ انتشار 2015-10-01
با دنبال کردن یک ژورنال هنگامی که شماره جدید این ژورنال منتشر می شود به شما از طریق ایمیل اطلاع داده می شود.
میزبانی شده توسط پلتفرم ابری doprax.com
copyright © 2015-2023